固溶(rong)(rong)(rong)(rong)處(chu)理(li)是(shi)將合(he)(he)金(jin)(jin)加熱到高(gao)溫單-相區恒溫保(bao)(bao)持(chi),使(shi)(shi)過(guo)(guo)(guo)(guo)剩相溶(rong)(rong)(rong)(rong)解(jie)到溶(rong)(rong)(rong)(rong)體后快速冷卻、以得到過(guo)(guo)(guo)(guo)飽(bao)和(he)(he)固溶(rong)(rong)(rong)(rong)體的(de)(de)(de)(de)(de)(de)熱處(chu)理(li)工藝。首先(xian),固溶(rong)(rong)(rong)(rong)處(chu)理(li)是(shi)為(wei)(wei)了(le)溶(rong)(rong)(rong)(rong)解(jie)基體內碳化物、γ'相等以得到均(jun)(jun)勻的(de)(de)(de)(de)(de)(de)過(guo)(guo)(guo)(guo)飽(bao)和(he)(he)固溶(rong)(rong)(rong)(rong)體,便于(yu)時(shi)(shi)效時(shi)(shi)重新析出(chu)顆粒細小(xiao)、分布(bu)均(jun)(jun)勻的(de)(de)(de)(de)(de)(de)碳化物和(he)(he)γ'等強化相,同時(shi)(shi)消(xiao)除(chu)由于(yu)冷熱加工產生的(de)(de)(de)(de)(de)(de)應力。使(shi)(shi)合(he)(he)金(jin)(jin)發生再結晶(jing)。其次,固溶(rong)(rong)(rong)(rong)處(chu)理(li)是(shi)為(wei)(wei)了(le)獲得適宜的(de)(de)(de)(de)(de)(de)晶(jing)粒度(du)(du)(du),以保(bao)(bao)證(zheng)合(he)(he)金(jin)(jin)高(gao)溫抗蠕(ru)變性(xing)能(neng)。固溶(rong)(rong)(rong)(rong)處(chu)理(li)的(de)(de)(de)(de)(de)(de)溫度(du)(du)(du)范圍為(wei)(wei)980~1250℃,主(zhu)要(yao)(yao)根據各個合(he)(he)金(jin)(jin)中相析出(chu)和(he)(he)溶(rong)(rong)(rong)(rong)解(jie)規律及使(shi)(shi)用(yong)要(yao)(yao)求(qiu)來選擇(ze),以保(bao)(bao)證(zheng)主(zhu)要(yao)(yao)強化相必要(yao)(yao)的(de)(de)(de)(de)(de)(de)析出(chu)條件和(he)(he)一定的(de)(de)(de)(de)(de)(de)晶(jing)粒度(du)(du)(du)。對(dui)于(yu)長(chang)期高(gao)溫使(shi)(shi)用(yong)的(de)(de)(de)(de)(de)(de)合(he)(he)金(jin)(jin),要(yao)(yao)求(qiu)有(you)較好的(de)(de)(de)(de)(de)(de)高(gao)溫持(chi)久(jiu)和(he)(he)蠕(ru)變性(xing)能(neng),應選擇(ze)較高(gao)的(de)(de)(de)(de)(de)(de)固溶(rong)(rong)(rong)(rong)溫度(du)(du)(du)以獲得較大的(de)(de)(de)(de)(de)(de)晶(jing)粒度(du)(du)(du);對(dui)于(yu)中溫使(shi)(shi)用(yong)并(bing)要(yao)(yao)求(qiu)較好的(de)(de)(de)(de)(de)(de)室(shi)溫硬度(du)(du)(du)、屈服強度(du)(du)(du)、拉伸強度(du)(du)(du)、沖擊韌性(xing)和(he)(he)疲勞強度(du)(du)(du)的(de)(de)(de)(de)(de)(de)合(he)(he)金(jin)(jin),可(ke)采用(yong)較低的(de)(de)(de)(de)(de)(de)固溶(rong)(rong)(rong)(rong)溫度(du)(du)(du),保(bao)(bao)證(zheng)較小(xiao)的(de)(de)(de)(de)(de)(de)晶(jing)粒度(du)(du)(du)。高(gao)溫固溶(rong)(rong)(rong)(rong)處(chu)理(li)時(shi)(shi),各種析出(chu)相都逐(zhu)步(bu)溶(rong)(rong)(rong)(rong)解(jie),同時(shi)(shi)晶(jing)粒長(chang)大;低溫固溶(rong)(rong)(rong)(rong)處(chu)理(li)時(shi)(shi),不僅有(you)主(zhu)要(yao)(yao)強化相的(de)(de)(de)(de)(de)(de)溶(rong)(rong)(rong)(rong)解(jie),而且可(ke)能(neng)有(you)某些相的(de)(de)(de)(de)(de)(de)析出(chu)。對(dui)于(yu)過(guo)(guo)(guo)(guo)飽(bao)和(he)(he)度(du)(du)(du)低的(de)(de)(de)(de)(de)(de)合(he)(he)金(jin)(jin),通常(chang)選擇(ze)較快的(de)(de)(de)(de)(de)(de)冷卻速度(du)(du)(du);對(dui)于(yu)過(guo)(guo)(guo)(guo)飽(bao)和(he)(he)度(du)(du)(du)高(gao)的(de)(de)(de)(de)(de)(de)合(he)(he)金(jin)(jin),通常(chang)為(wei)(wei)空氣中冷卻。
對2205雙(shuang)相不銹鋼(gang)進行不同溫度的固溶處理會導致2205雙相不銹(xiu)鋼(gang)兩相組織的改變,進而導致其性能的差異,圖3.1是在不同溫度下2205雙相不銹鋼固溶處理后的微觀組織。


選取1000℃作為(wei)(wei)最低(di)固溶溫(wen)度,當(dang)熱處理溫(wen)度低(di)于(yu)950℃時,雙相不銹鋼基體(ti)(ti)會析出雜質(zhi)相σ相,σ相作為(wei)(wei)富含Cr、Mo的硬(ying)脆相,其存在(zai)(zai)降低(di)雙相不銹鋼的耐蝕性能。圖(tu)3.1(a)為(wei)(wei)950℃的微(wei)觀組織,。相廣泛分布于(yu)鐵(tie)素(su)(su)體(ti)(ti)/奧氏體(ti)(ti)晶界。當(dang)溫(wen)度達到1000℃時,σ相會消失(shi),雙相不銹鋼中只存在(zai)(zai)鐵(tie)素(su)(su)體(ti)(ti)相和奧氏體(ti)(ti)相。圖(tu)3.1(b)~(f)中深色(se)區為(wei)(wei)鐵(tie)素(su)(su)體(ti)(ti),淺色(se)區為(wei)(wei)奧氏體(ti)(ti)。奧氏體(ti)(ti)以(yi)鐵(tie)素(su)(su)體(ti)(ti)為(wei)(wei)基體(ti)(ti),呈帶狀或島狀分布于(yu)鐵(tie)素(su)(su)體(ti)(ti)上。隨(sui)著(zhu)溫(wen)度的升高,奧氏體(ti)(ti)晶粒尺寸變大。
利(li)用IAS圖(tu)像(xiang)分(fen)析(xi)軟(ruan)件測量(liang)并計算(suan)相比(bi)例,每個熱處(chu)理溫(wen)(wen)度(du)下的(de)(de)金相圖(tu)取8張計算(suan),求取平均值。表3.2給(gei)出了利(li)用IAS圖(tu)像(xiang)分(fen)析(xi)軟(ruan)件計算(suan)得到(dao)(dao)不(bu)同固溶(rong)溫(wen)(wen)度(du)溫(wen)(wen)度(du)下2205雙相不(bu)銹鋼的(de)(de)相比(bi)例。1000℃時(shi),鐵(tie)素體(ti)(ti)含(han)量(liang)為48.3%,隨著固溶(rong)溫(wen)(wen)度(du)的(de)(de)升高,鐵(tie)素體(ti)(ti)相含(han)量(liang)增加,奧氏體(ti)(ti)相含(han)量(liang)下降(jiang),直到(dao)(dao)1200℃時(shi),鐵(tie)素體(ti)(ti)含(han)量(liang)達(da)到(dao)(dao)62.3%,奧氏體(ti)(ti)含(han)量(liang)僅占37.7%.這種(zhong)鐵(tie)素體(ti)(ti)與(yu)(yu)奧氏體(ti)(ti)隨固溶(rong)溫(wen)(wen)度(du)的(de)(de)變(bian)化(hua)規(gui)律前人的(de)(de)研究結果相一致(zhi)。兩(liang)相比(bi)例的(de)(de)變(bian)化(hua)曲線如圖(tu)3.2所示,兩(liang)相與(yu)(yu)溫(wen)(wen)度(du)的(de)(de)關系呈線性變(bian)化(hua)。當固溶(rong)溫(wen)(wen)度(du)約為1040℃時(shi),其(qi)相比(bi)例為1:1。


因(yin)此(ci)在本實(shi)驗的6個固溶(rong)溫度中,當固溶(rong)溫度為1050℃時,雙(shuang)相(xiang)不銹(xiu)鋼相(xiang)比(bi)例最接近1:1。
采用顯(xian)微(wei)硬度儀壓頭為菱(ling)形壓頭,荷載F為4.8N,分別測出菱(ling)形的兩個(ge)直徑d1和d2,根據下式計算顯(xian)微(wei)硬度:

所(suo)有(you)固溶(rong)溫(wen)度(du)試樣(yang)均測(ce)5個點,最(zui)后(hou)求取平均值(zhi)為個固溶(rong)溫(wen)度(du)下2205雙相不銹(xiu)鋼的顯(xian)(xian)微硬度(du)值(zhi)。顯(xian)(xian)微硬度(du)值(zhi)如表3.3所(suo)列,顯(xian)(xian)微硬度(du)隨固溶(rong)溫(wen)度(du)的變化曲線如圖3.3所(suo)示。
從圖3.3可知,2205雙相不銹鋼的顯微硬度先下降,后上升。這主要是由于當溫度為1000℃時,鐵素體相中間夾雜著小塊狀的二次奧氏體,當溫度達到1050℃后,二次奧氏體含量減少,組織均勻化程度提高,硬度減小。在此之后,隨著固溶溫度的增加,奧氏體含量減少,具有體心立方結構的奧氏體相屬于軟軔相,具有面心立方結構的鐵素體是強硬相,因此材料顯微硬度值又升高。同樣對2507雙相(xiang)不銹鋼進行不同溫度的固溶處理會導致2507雙相不銹鋼兩相組織的改變,進而導致其性能的差異,以下是2507雙相不銹鋼在不同溫度下固溶處理后的微觀組織。

2507雙相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不(bu)(bu)銹鋼分別在1000℃、1050℃、1100℃、1150℃、1200℃下(xia)固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)0.5h后水(shui)冷的(de)(de)(de)金(jin)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)組織如圖(tu)3.4所示。從圖(tu)3.4可以清晰地(di)得知(zhi)當(dang)固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)溫(wen)度(du)為1000℃時(shi)鐵素(su)(su)(su)體相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)與奧(ao)氏體相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)兩相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)界處(chu)(chu)(chu)有σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)析(xi)(xi)出,隨固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)處(chu)(chu)(chu)理(li)溫(wen)度(du)升(sheng)高到1050℃時(shi)σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)已經溶(rong)(rong)(rong)(rong)(rong)(rong)解。利(li)用Image-Pro-Plus 圖(tu)像分析(xi)(xi)儀(yi)軟件(jian)6.0版測定的(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比例如圖(tu)3.5所示。從圖(tu)3.5能夠獲得固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)處(chu)(chu)(chu)理(li)溫(wen)度(du)的(de)(de)(de)增高會導致(zhi)σ析(xi)(xi)出相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)含量降低,當(dang)固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)處(chu)(chu)(chu)理(li)溫(wen)度(du)大于(yu)1050℃時(shi)σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)已經完全(quan)溶(rong)(rong)(rong)(rong)(rong)(rong)解。這是由(you)于(yu)固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)處(chu)(chu)(chu)理(li)溫(wen)度(du)的(de)(de)(de)升(sheng)高使(shi)鋼中鐵素(su)(su)(su)體α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)量增多,導致(zhi)σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)形(xing)(xing)成元素(su)(su)(su)Cr和Mo在鐵素(su)(su)(su)體相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)中的(de)(de)(de)濃度(du)降低,進而導致(zhi)當(dang)固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)處(chu)(chu)(chu)理(li)溫(wen)度(du)大于(yu)1050℃時(shi)σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)的(de)(de)(de)形(xing)(xing)成受到抑(yi)制。考慮(lv)到σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)硬且脆,能夠大幅度(du)減弱材料的(de)(de)(de)塑(su)性與韌性,并且σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)富(fu)Cr,很容(rong)易在其周圍產生(sheng)貧Cr區(qu)降低DSS2507的(de)(de)(de)抗腐蝕性能,所以σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)為DSS2507析(xi)(xi)出相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)中危害最大的(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang),因此,在實際(ji)應(ying)用過(guo)程(cheng)中要想將2507雙相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不(bu)(bu)銹鋼中的(de)(de)(de)熱(re)軋態σ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)完全(quan)消除所選(xuan)用的(de)(de)(de)固(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)溫(wen)度(du)要不(bu)(bu)低于(yu)1050℃。


圖3.4中(zhong)深色(se)組(zu)(zu)織是(shi)鐵(tie)素體(ti)(ti)(ti)(ti)(ti)α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)、淺色(se)組(zu)(zu)織是(shi)奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)。從圖3.4可(ke)知奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)首先表現(xian)為(wei)長條狀,隨(sui)(sui)著(zhu)固(gu)(gu)(gu)溶(rong)(rong)(rong)處(chu)理溫(wen)度(du)的(de)(de)(de)(de)升高(gao)(gao)而(er)(er)逐(zhu)漸(jian)變(bian)短(duan),變(bian)成島(dao)狀分布在基(ji)體(ti)(ti)(ti)(ti)(ti)鐵(tie)素體(ti)(ti)(ti)(ti)(ti)上面。從圖3.5及表3.4中(zhong)給出的(de)(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比(bi)例(li)測(ce)量(liang)(liang)結果能夠獲得鋼(gang)中(zhong)鐵(tie)素體(ti)(ti)(ti)(ti)(ti)α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)量(liang)(liang)隨(sui)(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處(chu)理溫(wen)度(du)的(de)(de)(de)(de)升高(gao)(gao)而(er)(er)上升,奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)體(ti)(ti)(ti)(ti)(ti)積(ji)分數隨(sui)(sui)著(zhu)固(gu)(gu)(gu)溶(rong)(rong)(rong)溫(wen)度(du)的(de)(de)(de)(de)上升而(er)(er)下(xia)降(jiang),這(zhe)是(shi)由于在較高(gao)(gao)的(de)(de)(de)(de)固(gu)(gu)(gu)溶(rong)(rong)(rong)溫(wen)度(du)下(xia)2507雙相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不銹鋼(gang)呈現(xian)出的(de)(de)(de)(de)組(zu)(zu)織為(wei)單一的(de)(de)(de)(de)鐵(tie)素體(ti)(ti)(ti)(ti)(ti),隨(sui)(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處(chu)理溫(wen)度(du)的(de)(de)(de)(de)降(jiang)低(di)鐵(tie)素體(ti)(ti)(ti)(ti)(ti)逐(zhu)步(bu)轉(zhuan)化為(wei)奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)組(zu)(zu)織,即固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處(chu)理溫(wen)度(du)的(de)(de)(de)(de)升高(gao)(gao)導致(zhi)奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)逐(zhu)漸(jian)轉(zhuan)變(bian)為(wei)鐵(tie)素體(ti)(ti)(ti)(ti)(ti)組(zu)(zu)織。從圖3.5可(ke)以看出當固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處(chu)理溫(wen)度(du)在1000~1050℃之間(jian)時奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)y相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比(bi)例(li)減(jian)(jian)小(xiao)的(de)(de)(de)(de)比(bi)較緩慢,隨(sui)(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處(chu)理溫(wen)度(du)的(de)(de)(de)(de)升高(gao)(gao)奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)含(han)量(liang)(liang)減(jian)(jian)少的(de)(de)(de)(de)趨勢加快,這(zhe)是(shi)因為(wei)2507雙相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不銹鋼(gang)中(zhong)的(de)(de)(de)(de)氮元(yuan)素是(shi)奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)形(xing)成元(yuan)素,在較低(di)固(gu)(gu)(gu)溶(rong)(rong)(rong)溫(wen)度(du)下(xia)抑制了奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)向鐵(tie)素體(ti)(ti)(ti)(ti)(ti)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)的(de)(de)(de)(de)轉(zhuan)變(bian),而(er)(er)固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處(chu)理溫(wen)度(du)的(de)(de)(de)(de)升高(gao)(gao)會使(shi)N元(yuan)素穩定奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)的(de)(de)(de)(de)作用(yong)逐(zhu)漸(jian)減(jian)(jian)弱,進而(er)(er)導致(zhi)奧(ao)(ao)氏(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)向鐵(tie)素體(ti)(ti)(ti)(ti)(ti)α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)轉(zhuan)變(bian)速度(du)加快。
2507雙相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不(bu)銹鋼中(zhong)的(de)(de)(de)(de)奧氏(shi)體相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)和鐵素體相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)這(zhe)兩(liang)種(zhong)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)的(de)(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比(bi)例(li)主(zhu)要受固(gu)溶(rong)處(chu)(chu)理(li)(li)工藝以(yi)及自身化學成分的(de)(de)(de)(de)影(ying)響,當鋼的(de)(de)(de)(de)主(zhu)要化學成分確(que)定時(shi),則兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比(bi)例(li)與固(gu)溶(rong)處(chu)(chu)理(li)(li)制(zhi)度(du)有著(zhu)密切聯系。DSS2507的(de)(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比(bi)例(li)又(you)影(ying)響著(zhu)其自身的(de)(de)(de)(de)性能(neng)(neng)(neng)(neng)(neng),其塑性隨著(zhu)鐵素體含量的(de)(de)(de)(de)增多(duo)而(er)減弱、耐應(ying)力(li)腐(fu)蝕破裂(lie)能(neng)(neng)(neng)(neng)(neng)力(li)隨著(zhu)奧氏(shi)體含量升(sheng)高而(er)減弱,進(jin)而(er)認(ren)為當鐵素體α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)跟奧氏(shi)體γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)這(zhe)兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比(bi)例(li)接近(jin)(jin)1:1時(shi)雙相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不(bu)銹鋼的(de)(de)(de)(de)綜(zong)合性能(neng)(neng)(neng)(neng)(neng)最(zui)佳,有較好(hao)的(de)(de)(de)(de)抗腐(fu)蝕能(neng)(neng)(neng)(neng)(neng)力(li)以(yi)及較優的(de)(de)(de)(de)力(li)學性能(neng)(neng)(neng)(neng)(neng)。從(cong)圖3.5可(ke)知(zhi)固(gu)溶(rong)熱處(chu)(chu)理(li)(li)溫(wen)(wen)度(du)在(zai)1050~1100℃之(zhi)間時(shi)可(ke)以(yi)使鋼中(zhong)的(de)(de)(de)(de)兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)組織比(bi)例(li)達(da)(da)到(dao)1:1,本實(shi)驗中(zhong)所(suo)選用(yong)的(de)(de)(de)(de)5種(zhong)固(gu)溶(rong)溫(wen)(wen)度(du)中(zhong)1050℃時(shi)鐵素體α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)跟奧氏(shi)體γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比(bi)例(li)最(zui)接近(jin)(jin)1:1,進(jin)而(er)可(ke)以(yi)認(ren)為選擇較優的(de)(de)(de)(de)固(gu)溶(rong)熱處(chu)(chu)理(li)(li)溫(wen)(wen)度(du)使DSS2507中(zhong)的(de)(de)(de)(de)兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)含量比(bi)例(li)達(da)(da)到(dao)1:1是有可(ke)能(neng)(neng)(neng)(neng)(neng)的(de)(de)(de)(de),在(zai)實(shi)際應(ying)用(yong)過程中(zhong)為了使2507雙相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不(bu)銹鋼獲得較好(hao)的(de)(de)(de)(de)綜(zong)合性能(neng)(neng)(neng)(neng)(neng),進(jin)行固(gu)溶(rong)處(chu)(chu)理(li)(li)時(shi)選取(qu)的(de)(de)(de)(de)固(gu)溶(rong)溫(wen)(wen)度(du)應(ying)該在(zai)1050~1100℃之(zhi)間。
2507雙相(xiang)(xiang)(xiang)不(bu)銹鋼(gang)分別(bie)在1000℃、1050℃、1100℃、1150℃、1200℃固溶(rong)(rong)0.5h后水冷的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)值如圖3.6所(suo)示。從圖3.6可知(zhi)DSS2507的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)隨(sui)(sui)(sui)固溶(rong)(rong)處(chu)理(li)(li)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)的(de)(de)(de)升(sheng)(sheng)(sheng)高先減小后變大呈曲線變化。在1000~1050℃溫(wen)(wen)(wen)(wen)(wen)度(du)(du)范(fan)(fan)圍(wei)內鋼(gang)的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)隨(sui)(sui)(sui)固溶(rong)(rong)熱(re)處(chu)理(li)(li)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)的(de)(de)(de)增(zeng)高而(er)逐漸(jian)減小,1050~1200℃范(fan)(fan)圍(wei)內隨(sui)(sui)(sui)固溶(rong)(rong)熱(re)處(chu)理(li)(li)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)的(de)(de)(de)上升(sheng)(sheng)(sheng)硬(ying)(ying)(ying)度(du)(du)又漸(jian)漸(jian)變大,且1050℃時(shi)DSS2507的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)表現為最小。從3.2.1節分析(xi)可知(zhi)當(dang)固溶(rong)(rong)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)為1000℃時(shi)在鐵素(su)(su)體(ti)(ti)和奧氏體(ti)(ti)相(xiang)(xiang)(xiang)界處(chu)有(you)σ相(xiang)(xiang)(xiang)析(xi)出(chu),σ相(xiang)(xiang)(xiang)是(shi)一種(zhong)硬(ying)(ying)(ying)而(er)脆的(de)(de)(de)相(xiang)(xiang)(xiang),能夠提高雙相(xiang)(xiang)(xiang)不(bu)銹鋼(gang)的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)值,所(suo)以(yi)1000℃下(xia)(xia)鋼(gang)有(you)較高的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du),而(er)σ相(xiang)(xiang)(xiang)會隨(sui)(sui)(sui)固溶(rong)(rong)熱(re)處(chu)理(li)(li)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)的(de)(de)(de)升(sheng)(sheng)(sheng)高而(er)漸(jian)漸(jian)溶(rong)(rong)解(jie)到(dao)基體(ti)(ti)中(zhong),DSS2507的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)有(you)下(xia)(xia)降(jiang)的(de)(de)(de)趨勢;同(tong)時(shi)又由于(yu)固溶(rong)(rong)熱(re)處(chu)理(li)(li)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)的(de)(de)(de)增(zeng)高導致鋼(gang)中(zhong)的(de)(de)(de)鐵素(su)(su)體(ti)(ti)相(xiang)(xiang)(xiang)量(liang)增(zeng)加而(er)奧氏體(ti)(ti)相(xiang)(xiang)(xiang)量(liang)降(jiang)低,在室(shi)溫(wen)(wen)(wen)(wen)(wen)下(xia)(xia)鐵素(su)(su)體(ti)(ti)是(shi)體(ti)(ti)心立方(fang)結構(gou)(bcc)奧氏體(ti)(ti)是(shi)面心立方(fang)結構(gou)(fcc),前者硬(ying)(ying)(ying)度(du)(du)要高于(yu)后者,因此在鐵素(su)(su)體(ti)(ti)含量(liang)逐漸(jian)升(sheng)(sheng)(sheng)高的(de)(de)(de)情況下(xia)(xia)鋼(gang)的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)也逐漸(jian)升(sheng)(sheng)(sheng)高,即隨(sui)(sui)(sui)著固溶(rong)(rong)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)的(de)(de)(de)升(sheng)(sheng)(sheng)高2507 雙相(xiang)(xiang)(xiang)不(bu)銹鋼(gang)的(de)(de)(de)硬(ying)(ying)(ying)度(du)(du)呈升(sheng)(sheng)(sheng)高的(de)(de)(de)趨勢。綜上所(suo)述,隨(sui)(sui)(sui)固溶(rong)(rong)溫(wen)(wen)(wen)(wen)(wen)度(du)(du)從1000℃上升(sheng)(sheng)(sheng)到(dao)1200℃,2507雙相(xiang)(xiang)(xiang)不(bu)銹鋼(gang)硬(ying)(ying)(ying)度(du)(du)呈先降(jiang)低后升(sheng)(sheng)(sheng)高的(de)(de)(de)變化趨勢。


